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Headspace gas chromatography uses headspace gas—from the top or "head" of a sealed container containing a liquid or solid brought to equilibrium [1] —injected directly onto a gas chromatographic column for separation and analysis.
Gas chromatography (GC) is a common type of chromatography used in analytical chemistry for separating and analyzing compounds that can be vaporized without decomposition. Typical uses of GC include testing the purity of a particular substance, or separating the different components of a mixture. [ 1 ]
English: Schematic drawing of the headspace analysis in gas chromatography. After thermal equilibration, a sample is taken out of the headspace and the analytical compounds are seperated and identified on the GC column. Main advantage: Even with complex sample matrices (e.g. blood, honey), the GC column is not contaminated with sample components.
The target analytes are extracted by mixing the sample with water and purge with inert gas (e.g. Nitrogen gas) into an airtight chamber, this is known as purging or sparging. The volatile compounds move into the headspace above the water and are drawn along a pressure gradient (caused by the introduction of the purge gas) out of the chamber ...
Headspace technology is a technique developed in the 1980s to elucidate the odor ... The samples can then be analyzed using techniques such as gas chromatography, ...
Headspace or ullage, the unfilled space in a container; Headspace technology, the gaseous constituents of a closed space above liquids or solid emitting and vapors measured using headspace gas chromatography; Headspace (firearms), a chamber measurement; Headroom (photographic framing), a concept of aesthetic composition in imaging
Included are detailed explanations for numerous common analytical methods such as gas, liquid, ion, and headspace chromatography, atomic absorption spectroscopy, and optical emission spectroscopy. Reagent Chemicals is primarily of interest to manufacturers and suppliers of chemicals to laboratories worldwide, and less so to research ...
Analytical thermal desorption, known within the analytical chemistry community simply as "thermal desorption" (TD), is a technique that concentrates volatile organic compounds (VOCs) in gas streams prior to injection into a gas chromatograph (GC). It can be used to lower the detection limits of GC methods, and can improve chromatographic ...