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An evaporating dish is a piece of laboratory glassware used for the evaporation of solutions and supernatant liquids, [a] and sometimes to their melting point.Evaporating dishes are used to evaporate excess solvents – most commonly water – to produce a concentrated solution or a solid precipitate of the dissolved substance.
A Kugelrohr (German for "ball tube") is a short-path vacuum distillation apparatus [1]: 150 typically used to distill relatively small amounts of compounds with high boiling points (usually greater than 300 °C) under greatly reduced pressure.
Vacuum Sugar Apparatus at The Great Exhibition, 1851. Vacuum evaporation is the process of causing the pressure in a liquid-filled container to be reduced below the vapor pressure of the liquid, causing the liquid to evaporate at a lower temperature than normal.
Evaporation takes place in a vacuum, i.e. vapors other than the source material are almost entirely removed before the process begins. In high vacuum (with a long mean free path), evaporated particles can travel directly to the deposition target without colliding with the background gas. (By contrast, in the boiling pot example, the water vapor ...
Therefore, placing a solution under reduced pressure makes the dissolved gas less soluble. Sonication and stirring under reduced pressure can usually enhance the efficiency. This technique is often referred to as vacuum degasification. Specialized vacuum chambers, called vacuum degassers, are used to degas materials through pressure reduction.
Because the cooling water, which is chemically treated fresh water, is at a temperature of 70–80 °C (158–176 °F), it would not be possible to flash off any water vapor unless the pressure in the heat exchanger vessel is dropped. A brine-air ejector venturi pump is then used to create a vacuum inside the vessel, achieving partial evaporation.
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