Ads
related to: drying thf with molecular sievesmart.ecer.com has been visited by 10K+ users in the past month
Search results
Results From The WOW.Com Content Network
Commercial THF contains substantial water that must be removed for sensitive operations, e.g. those involving organometallic compounds. Although THF is traditionally dried by distillation from an aggressive desiccant such as elemental sodium, molecular sieves have been shown to be superior water scavengers. [20]
3A molecular sieves are used to dry a range of materials, such as ethanol, air, refrigerants, natural gas and unsaturated hydrocarbons. The latter include cracking gas, acetylene, ethylene, propylene and butadiene. 3A molecular sieves are stored at room temperature, with a relative humidity not more than 90%. They are sealed under reduced ...
2-Methyltetrahydrofuran (2-MeTHF) is an organic compound with the molecular formula C 5 H 10 O. It is a highly flammable, mobile liquid. It is mainly used as a replacement for Tetrahydrofuran (THF) in specialized applications for its better performance, such as to obtain higher reaction temperatures, or easier separations (as, unlike THF, it is not miscible with water).
Anhydrous sodium carbonate can be used as an "in bottle" drying agent for anhydrous THF, as it is not sufficiently nucleophilic to react. To be any use, the sodium carbonate has to be freshñly dried: actually, it's not that common these days, as most people who want really dry THF distill it directly from sodium benzophenone ketyl, but I think ...
Canisters are commonly filled with silica gel and other molecular sieves as desiccants in drug containers to keep contents dry Silica gel in a sachet or porous packet. A desiccant is a hygroscopic substance that is used to induce or sustain a state of dryness (desiccation) in its vicinity; it is the opposite of a humectant.
Size-exclusion chromatography, also known as molecular sieve chromatography, [1] is a chromatographic method in which molecules in solution are separated by their shape, and in some cases size. [2] It is usually applied to large molecules or macromolecular complexes such as proteins and industrial polymers . [ 3 ]