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Crucibles used in Czochralski method Melting gold in a graphite crucible Three crucibles used by Thomas Edison. Crucibles are used in the laboratory to contain chemical compounds when they are heated to extremely high temperatures. Crucibles are available in several sizes and typically come with a correspondingly-sized lid. [20]
16th century cupellation furnaces (per Agricola). Cupellation is a refining process in metallurgy in which ores or alloyed metals are treated under very high temperatures and subjected to controlled operations to separate noble metals, like gold and silver, from base metals, like lead, copper, zinc, arsenic, antimony, or bismuth, present in the ore.
Charging of the crucible with starting materials (mixture of powders) Heating of the crucible until starting materials in the crucible are completely melted; Upward displacement of the seed until its contact with the meniscus or crucible; Formation of the meniscus and partial melting of the seed top
One process for X-ray fluorescence assay involves melting the material in a furnace and stirring to make a homogeneous mix. Following this, a sample is taken from the centre of the molten sample. Samples are typically taken using a vacuum pin tube. [4] The sample is then tested by X-ray fluorescence spectroscopy. Metallurgical assay is ...
The process can be carried out in a horizontal or vertical orientation, and usually involves a rotating crucible/ampoule to stir the melt. [ 1 ] The Bridgman method is a popular way of producing certain semiconductor crystals such as gallium arsenide , for which the Czochralski method is more difficult.
In contrast to the use of mercury (which relies on amalgamation of the gold to coalesce it and separate it from impurities) this method relies on borax's ability to lower all the minerals' melting points. Since the gold is usually the heaviest of these minerals, it allows for concentrating the gold on the bottom of the crucible.