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An X-cut is made through the film with a carbide tip tool to the substrate. Pressure-sensitive tape is applied over the cut. Tape is smoothed into place using a pencil eraser over the area of the incisions. Tape is removed by pulling it off rapidly back over itself as close to an angle of 180°. Adhesion is assessed on a 0 to 5 scale.
The scale was defined by Albert Ferdinand Shore, who developed a suitable device to measure hardness in the 1920s. It was neither the first hardness tester nor the first to be called a durometer ( ISV duro- and -meter ; attested since the 19th century), but today that name usually refers to Shore hardness ; other devices use other measures ...
Surface roughness can also affect the adhesive strength. Surfaces with roughness on the scale of 1–2 micrometres can yield better wetting because they have a larger surface area. Thus, more intermolecular interactions at closer distances can arise, yielding stronger attractions and larger adhesive strength.
Bloom is a test used to measure the strength of a gel, most commonly gelatin.The test was originally developed and patented in 1925 by Oscar T. Bloom. [1] The test determines the weight in grams needed by a specified plunger (normally with a diameter of 0.5 inch) to depress the surface of the gel by 4 mm without breaking it at a specified temperature. [2]
The breakdown of polymer chains is often undetectable until the adhesive has reached a critical point where the stability of remainder of the adhesive rapidly degrades. [1] High temperature accelerated testing often cannot be used to estimate stability in oxygen environments since high temperatures often lead to new reaction pathways that would ...
The success or failure of the bond is based on measuring the applied force, the failure type due to the applied force and the visual appearance of the residual medium used. A development in bond strength testing of adhesively bonded composite structures is laser bond inspection (LBI). LBI provides a relative strength quotient derived from the ...
Adhesive materials fill the voids or pores of the surfaces and hold surfaces together by interlocking. Other interlocking phenomena are observed on different length scales. Sewing is an example of two materials forming a large scale mechanical bond, velcro forms one on a medium scale, and some textile adhesives (glue) form one at a small scale.
Pressure-sensitive adhesives are designed with a balance between flow and resistance to flow. The bond forms because the adhesive is soft enough to flow, or wet, the adherend. The bond has strength because the adhesive is hard enough to resist flow when stress is applied to the bond.