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Zinc dust was then stirred in, reducing the oxime group to the amine. This reduction consumes two equivalents of zinc and four equivalents of acetic acid. Knorr 1886 synthesis. Modern practice is to add the oxime solution resulting from the nitrosation and the zinc dust gradually to a well-stirred solution of ethyl acetoacetate in glacial ...
Metal fume fever, also known as brass founders' ague, brass shakes, [1] zinc shakes, galvie flu, galvo poisoning, metal dust fever, welding shivers, or Monday morning fever, [2] is an illness primarily caused by exposure to chemicals such as zinc oxide (ZnO), aluminium oxide (Al 2 O 3), or magnesium oxide (MgO) which are produced as byproducts in the fumes that result when certain metals are ...
The Waelz process is a method of recovering zinc and other relatively low boiling point metals from metallurgical waste (typically electric arc furnace flue dust) and other recycled materials using a rotary kiln (waelz kiln). The zinc enriched product is referred to as waelz oxide, and the reduced zinc by product as waelz slag.
It forms on the surface of low-melting-point metals such as tin, lead, zinc or aluminium or alloys by oxidation of the metal. For higher melting point metals and alloys such as steel and silver, oxidized impurities melt and float making them easy to pour off. With wrought iron, hammering and later rolling remove some dross. [1]
The Merrill–Crowe Process is a separation technique for removing gold from the solution obtained by the cyanide leaching of gold ores. It is an improvement of the MacArthur-Forrest process, where an additional vacuum is managed to remove air in the solution (invention of Crowe), and zinc dust is used instead of zinc shavings (improvement of Merrill).
Raney nickel, platinum on carbon, or zinc dust and formic acid or ammonium formate [6] α,β-Unsaturated nitro compounds can be reduced to saturated amines by: Catalytic hydrogenation over palladium-on-carbon; Iron metal; Lithium aluminium hydride [27] (Note: Hydroxylamines and oximes are typical impurities.)
Zinc is extracted from the purified zinc sulfate solution by electrowinning, which is a specialized form of electrolysis. The process works by passing an electric current through the solution in a series of cells. This causes the zinc to deposit on the cathodes (aluminium sheets) and oxygen to form at the anodes. Sulfuric acid is also formed in ...
Zinc sulfate is an inorganic compound with the formula ZnSO 4.It forms hydrates ZnSO 4 ·nH 2 O, where n can range from 0 to 7. All are colorless solids. The most common form includes water of crystallization as the heptahydrate, [4] with the formula Zn SO 4 ·7H 2 O.