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For the polymer chemist, DSC is a handy tool for studying curing processes, which allows the fine tuning of polymer properties. The cross-linking of polymer molecules that occurs in the curing process is exothermic, resulting in a negative peak in the DSC curve that usually appears soon after the glass transition.
The Barcol hardness test is generally used on soft materials such as rigid plastics. It measures hardness based on indentation of a sharp point with a flat tip. The test is performed using a similar method and indentation device as that used to measure Shore D hardness, however the Shore D indentor has a round tip. [4]
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For investigation of the curing behavior of thermosetting resin systems, composite materials, adhesives and paints, Dielectric Analysis (DEA) can be used in accordance with ASTM E 2038 or E 2039. The great advantage of DEA is that it can be employed not only on a laboratory scale, but also in process.
Polymers represent another large area in which thermal analysis finds strong applications. Thermoplastic polymers are commonly found in everyday packaging and household items, but for the analysis of the raw materials, effects of the many additive used (including stabilisers and colours) and fine-tuning of the moulding or extrusion processing used can be achieved by using differential scanning ...
Figure 4: Evolution in time of storage modulus G' and loss modulus G" during a curing reaction. A simple way to monitor the change in viscosity, and thus, the extent of the reaction, in a curing process is to measure the variation of the elastic modulus. [7] To measure the elastic modulus of a system during curing, a rheometer can be used. [7]
Characteristic DSC curve for a polyethylene, the OIT is measured. Oxidation induction time or OIT is a standardized test performed in a DSC which measures the level of thermal stabilization of the material tested. The time between melting and the onset of decomposition in isothermal conditions is measured.
In the bullion fire assay process, a sample from the article is wrapped in a lead foil with copper and silver. The wrapped sample, along with prepared control samples, heated at 1,650 °F (or 898.9 °C; temperature varies with exact method) in a cupel made of compressed bone ash or magnesium oxide powder.