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A McCabe–Thiele diagram for the distillation of a binary (two-component) feed is constructed using the vapor-liquid equilibrium (VLE) data—which is how vapor is concentrated when in contact with its liquid form—for the component with the lower boiling point. Figure 1: Typical McCabe–Thiele diagram for distillation of a binary feed
Distillation Design is a book which provides complete coverage of the design of industrial distillation columns for the petroleum refining, chemical and petrochemical plants, natural gas processing, pharmaceutical, food and alcohol distilling industries.
In this case the mixture components A and B are separated in the first column through the solvent E (recovered in the second column). Extractive distillation is defined as distillation in the presence of a miscible , high-boiling, relatively non-volatile component, the solvent , that forms no azeotrope with the other components in the mixture.
An overhead condenser is a heat exchange equipment used for condensing the mixture leaving the top of the column. Either cooling water or air is used as a cooling agent. An overhead accumulator is a horizontal pressure vessel containing the condensed mixture. Pumps can be used to control the reflux to the column.
N t is then divided by the tray efficiency, E, to determine the actual number of trays or physical plates, N a, needed in the separating column. The final design choice of the number of trays to be installed in an industrial distillation column is then selected based upon an economic balance between the cost of additional trays and the cost of ...
Schematics of a plate column with bubble cap trays. The feed to the column can be liquid, gas or gas and liquid at equilibrium. Inside the column there are always two phases: one gas phase and one liquid phase. The liquid phase flows downward through the column via gravity, [1] while the gas phase flows upward.
Fractionation at total reflux. The Fenske equation in continuous fractional distillation is an equation used for calculating the minimum number of theoretical plates required for the separation of a binary feed stream by a fractionation column that is being operated at total reflux (i.e., which means that no overhead product distillate is being withdrawn from the column).
Modeling and simulation of batch distillation unit is done with the help of one of the most important process simulators (aspen plus) used in chemical industry with the following data given in the table and check the simulation result. Various steps are involved in the simulation of batch distillation column using aspen plus software is :