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Solid-phase microextraction (SPME), is a solid phase extraction technique that involves the use of a fiber coated with an extracting phase, that can be a liquid or a solid , which extracts different kinds of analytes (including both volatile and non-volatile) from different kinds of media, that can be in liquid or gas phase. [9]
Laboratory-scale liquid-liquid extraction. Photograph of a separatory funnel in a laboratory scale extraction of 2 immiscible liquids: liquids are a diethyl ether upper phase, and a lower aqueous phase. Soxhlet extractor. Extraction in chemistry is a separation process consisting of the separation of a substance from a matrix. The distribution ...
Evaporation removes volatile liquids from non-volatile solutes, which cannot be done through filtration due to the small size of the substances. Liquid–liquid extraction removes an impurity or recovers a desired product by dissolving the crude material in a solvent in which other components of the feed material are soluble.
Solid-phase microextraction sampling. Solid phase microextraction, or SPME, is a solid phase extraction sampling technique that involves the use of a fiber coated with an extracting phase, that can be a liquid or a solid (), [1] which extracts different kinds of analytes (including both volatile and non-volatile) from different kinds of media, that can be in liquid or gas phase. [2]
Demister (vapor), removes liquid droplets from gas streams; Distillation, used for mixtures of liquids with different boiling points; Drying, removes liquid from a solid by vaporization or evaporation; Electrophoresis, separates organic molecules based on their different interaction with a gel under an electric potential (i.e., different travel)
It was originally designed for the extraction of a lipid from a solid material. Typically, Soxhlet extraction is used when the desired compound has a limited solubility in a solvent, and the impurity is insoluble in that solvent. It allows for unmonitored and unmanaged operation while efficiently recycling a small amount of solvent to dissolve ...
A more common definition is that "Absorption is a chemical or physical phenomenon in which the molecules, atoms and ions of the substance getting absorbed enter into the bulk phase (gas, liquid or solid) of the material in which it is taken up." A more general term is sorption, which covers absorption, adsorption, and ion exchange. Absorption ...
[note 1] While the chaotropic effect was previously known and reported by other scientists, [10] [note 2] Boom et al. contributed an optimization of the method to complex starting materials, [1] such as body fluids and other biological starting materials, and provided a short procedure according to the Boom et al. US5234809. [1]