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A blank value in analytical chemistry is a measurement of a blank. The reading does not originate from a sample, but the matrix effects , reagents and other residues . These contribute to the sample value in the analytical measurement and therefore have to be subtracted.
A blank solution is a solution containing little to no analyte of interest, [1] usually used to calibrate instruments such as a colorimeter. According to the EPA, the "primary purpose of blanks is to trace sources of artificially introduced contamination." [2] Different types of blanks are used to identify the source of contamination in the ...
Most analytical instruments produce a signal even when a blank (matrix without analyte) is analyzed.This signal is referred to as the noise level. The instrument detection limit (IDL) is the analyte concentration that is required to produce a signal greater than three times the standard deviation of the noise level.
Since most analytical instrumentation is comparative, it requires a sample of known composition (reference material) for accurate calibration. These reference materials are produced under stringent manufacturing procedures and differ from laboratory reagents in their certification and the traceability of the data provided.
An assay (analysis) is never an isolated process, as it must be accompanied with pre- and post-analytic procedures. Both the communication order (the request to perform an assay plus related information) and the handling of the specimen itself (the collecting, documenting, transporting, and processing done before beginning the assay) are pre-analytic steps.
A microscope slide prepared in 1855 containing reference specimens from the inner mucosa of the small intestine of a cholera victim.. The origin of the concept was pieces of ivory or bone, containing specimens held between disks of transparent mica, that would slide into the gap between the stage and the objective. [1]
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The check sheet is a form (document) used to collect data in real time at the location where the data is generated. The data it captures can be quantitative or qualitative. When the information is quantitative, the check sheet is sometimes called a tally sheet. [1] The check sheet is one of the so-called Seven Basic Tools of Quality Control. [2]