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Chlorine can be manufactured by the electrolysis of a sodium chloride solution , which is known as the Chloralkali process. The production of chlorine results in the co-products caustic soda (sodium hydroxide, NaOH) and hydrogen gas (H 2). These two products, as well as chlorine itself, are highly reactive.
The reaction at anode (A) is: 2 Cl − → Cl 2 + 2 e −. The chlorine gas that results vents at the top of the outside cells where it is collected as a byproduct of the process. The reaction at the mercury cathode in the outer cells is Na + + e − → Na (amalgam) The sodium metal formed by this reaction dissolves in the mercury to form an ...
Potassium chloride is inexpensively available and is rarely prepared intentionally in the laboratory. It can be generated by treating potassium hydroxide (or other potassium bases) with hydrochloric acid: KOH + HCl → KCl + H 2 O. This conversion is an acid-base neutralization reaction. The resulting salt can then be purified by recrystallization.
The process has a high energy consumption, for example around 2,500 kWh (9,000 MJ) of electricity per tonne of sodium hydroxide produced. Because the process yields equivalent amounts of chlorine and sodium hydroxide (two moles of sodium hydroxide per mole of chlorine), it is necessary to find a use for these products in the same proportion ...
Potassium hypochlorite is produced by the disproportionation reaction of chlorine with a solution of potassium hydroxide: [2] Cl 2 + 2 KOH → KCl + KOCl + H 2 O. This is the traditional method, first used by Claude Louis Berthollet in 1789. [3] Another production method is electrolysis of potassium chloride solution.
The cathode reaction is 2 Na + + 2 e − → 2Na. The anode reaction is 4 OH − → O 2 + 2 H 2 O + 4 e −. Despite the elevated temperature, some of the water produced remains dissolved in the electrolyte. [4] This water diffuses throughout the electrolyte and results in the reverse reaction taking place on the electrolyzed sodium metal:
Cannizzaro first accomplished this transformation in 1853, when he obtained benzyl alcohol and potassium benzoate from the treatment of benzaldehyde with potash (potassium carbonate). More typically, the reaction would be conducted with sodium hydroxide or potassium hydroxide , giving the sodium or potassium carboxylate salt of the carboxylic ...
Dichlorocarbene is an intermediate in the carbylamine reaction. In this conversion, a dichloromethane solution of a primary amine is treated with chloroform and aqueous sodium hydroxide in the presence of catalytic amount of the phase-transfer catalyst. Illustrative is the synthesis of tert-butyl isocyanide: [7]