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  2. Sample preparation in mass spectrometry - Wikipedia

    en.wikipedia.org/wiki/Sample_preparation_in_mass...

    Sample preparation for mass spectrometry is used for the optimization of a sample for analysis in a mass spectrometer (MS). Each ionization method has certain factors that must be considered for that method to be successful, such as volume, concentration, sample phase, and composition of the analyte solution. Quite possibly the most important ...

  3. Standard solution - Wikipedia

    en.wikipedia.org/wiki/Standard_solution

    Standard solutions are generally prepared by dissolving a solute of known mass into a solvent to a precise volume, or by diluting a solution of known concentration with more solvent. [1] A standard solution ideally has a high degree of purity and is stable enough that the concentration can be accurately measured after a long shelf time. [2]

  4. Gas chromatography–mass spectrometry - Wikipedia

    en.wikipedia.org/wiki/Gas_chromatography–mass...

    GCMS is used for the analysis of unknown organic compound mixtures. One critical use of this technology is the use of GCMS to determine the composition of bio-oils processed from raw biomass. [29] GCMS is also utilized in the identification of continuous phase component in a smart material, magnetorheological (MR) fluid. [30]

  5. Two-dimensional chromatography - Wikipedia

    en.wikipedia.org/wiki/Two-dimensional_chromatography

    Gas chromatography-mass spectrometry (GC-MS) is a two-dimensional chromatography technique that combines the separation technique of gas chromatography with the identification technique of mass spectrometry. GC-MS is the single most important analytical tool for the analysis of volatile and semi-volatile organic compounds in complex mixtures. [7]

  6. Direct electron ionization liquid chromatography–mass ...

    en.wikipedia.org/wiki/Direct_electron_ionization...

    The interfacing mechanism is contained inside a common EI source, like that found in any GC-MS system. The liquid phase from a nano HPLC column is admitted from the capillary column port, where the connection tubing and the nebulizer are first introduced and sealed to prevent vacuum loss.

  7. Desorption electrospray ionization - Wikipedia

    en.wikipedia.org/wiki/Desorption_electrospray...

    Schematic diagram of the DESI ion source. Desorption electrospray ionization (DESI) is an ambient ionization technique that can be coupled to mass spectrometry (MS) for chemical analysis of samples at atmospheric conditions. Coupled ionization sources-MS systems are popular in chemical analysis because the individual capabilities of various ...

  8. Capillary electrophoresis–mass spectrometry - Wikipedia

    en.wikipedia.org/wiki/Capillary_electrophoresis...

    Schematic diagram of online CE-MALDI-MS. Off-line coupling of CE to MALDI, the CE effluent could be sprayed or added drop wise on MALDI target plate then dried and analyzed by MS. For online coupling, a moving target with continuous contact to CE capillary end is required. The moving target takes analytes into MS where it is desorbed and ionized.

  9. Pyrolysis GC/MS chromatogram of mahogany wood analyzed with OpenChrom. Pyrolysis–gas chromatography–mass spectrometry is a method of chemical analysis in which the sample is heated to decomposition to produce smaller molecules that are separated by gas chromatography and detected using mass spectrometry. [1] [2]