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The Schlenk line (also vacuum gas manifold) is a commonly used chemistry apparatus developed by Wilhelm Schlenk. [1] It consists of a dual manifold with several ports. [ 2 ] One manifold is connected to a source of purified inert gas , while the other is connected to a vacuum pump .
Argon is often used when analysing gas phase chemistry reactions such as F-T synthesis so that a single carrier gas can be used rather than two separate ones. The sensitivity is reduced, but this is a trade off for simplicity in the gas supply. Gas chromatography is used extensively in forensic science. Disciplines as diverse as solid drug dose ...
Frequently, steam, air, inert gases, and hydrocarbon gases are used as stripping agents. This is based on solubility, stability, degree of corrosiveness, cost, and availability. As stripping agents are gases, operation at nearly the highest temperature and lowest pressure that will maintain the components and not vaporize the liquid feed stream ...
Bubbling a solution with a high-purity (typically inert) gas can pull out undesired (typically reactive) dissolved gases such as oxygen and carbon dioxide. Nitrogen, argon, helium and other inert gases are commonly used. To maximize this process called sparging, the solution is stirred vigorously and bubbled for a long time.
Gas bubblers are used to exclude air from a reaction or a system. In the former case, the gas bubbler is fitted on the condenser of the reaction set-up. In the latter case, an oil bubbler is usually installed at the end of the inert gas manifold on a Schlenk line to prevent contamination by atmospheric oxygen and water .
The term inert gas is context-dependent because several of the inert gases, including nitrogen and carbon dioxide, can be made to react under certain conditions. [ 1 ] [ 2 ] Purified argon gas is the most commonly used inert gas due to its high natural abundance (78.3% N 2 , 1% Ar in air) [ 3 ] and low relative cost.
The design of the flame ionization detector varies from manufacturer to manufacturer, but the principles are the same. Most commonly, the FID is attached to a gas chromatography system. The eluent exits the gas chromatography column (A) and enters the FID detector’s oven (B). The oven is needed to make sure that as soon as the eluent exits ...
Sparging introduces a gas that has little or no partial pressure of the gas(es) to be removed, and increases the area of the gas-liquid interface, which encourages some of the dissolved gas(es) to diffuse into the sparging gas before the sparging gas escapes from the liquid. Many sparging processes, such as solvent removal, use air as the ...