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As the mixture is heated and boils, vapor rises up the column. The vapor condenses on the glass platforms (known as plates or trays) inside the column and runs back down into the liquid below, thereby refluxing the upflowing distillate vapor. The hottest tray is at the bottom of the column and the coolest tray is at the top.
A liquid (not visible) in the flask at left is heated by the blue mantle to the boiling point. The vapor is then cooled as it goes through the inner tube of the condenser. There it becomes liquid again, and drips into the smaller collecting flask at right, immersed in a cooling bath. The two hoses connected to the condenser circulate water ...
Flat-bottomed flask: A flask with similar uses as the round-bottom flask, but with a flat bottom that allows it to stand on a level surface. Florence flask: A flask similar to the flat-bottomed flask that has round bodies and either a round bottom or a flat bottom so that one can stand the flask on a level surface. Florence flasks typically ...
The non-soluble portion of the extracted solid remains in the thimble, and is usually discarded. Like Soxhlet extractor, the Kumagawa extractor has a specific design where the thimble holder/chamber is directly suspended inside the solvent flask (having a vertical large opening) above the boiling solvent.
For example, a round bottom flask, Liebig condenser, and oil bubbler with ground glass joints may be rapidly fitted together to reflux a reaction mixture. This is a large improvement compared with older methods of custom-made glassware, which was time-consuming and expensive, or the use of less chemical resistant and heat resistant corks or ...
A Florence flask has a round body, a long neck, and often a flat bottom. It is designed for uniform heating, boiling, distillation and ease of swirling; it is produced in a number of different glass thicknesses to stand different types of use.
In a typical fractional distillation, a liquid mixture is heated in the distilling flask, and the resulting vapor rises up the fractionating column (see Figure 1). The vapor condenses on glass spurs (known as theoretical trays or theoretical plates) inside the column, and returns to the distilling flask, refluxing the rising distillate vapor ...
It is used in combination with a reflux condenser and a distillation flask for the separation of water from liquids. This may be a continuous removal of the water that is produced during a chemical reaction performed at reflux temperature, such as in esterification reactions. The original setup by Julius Marcusson (invented in 1905) was refined ...