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Distillation setup using a retort and tube condenser, from a 1921 book. [5] The simplest type of condenser is a straight tube, cooled only by the surrounding air. The tube is held in a vertical or oblique position, and the vapor is fed through the upper end. The heat of condensation is carried away by convection.
Like vacuum distillation, steam distillation is a method for distilling compounds which are heat-sensitive. [ 1 ] : 151–153 The temperature of the steam is easier to control than the surface of a heating element and allows a high rate of heat transfer without heating at a very high temperature.
A condenser is designed to transfer heat from a working fluid (e.g. water in a steam power plant) to a secondary fluid or the surrounding air. The condenser relies on the efficient heat transfer that occurs during phase changes, in this case during the condensation of a vapor into a liquid. The vapor typically enters the condenser at a ...
The purpose is to thermally accelerate the reaction by conducting it at an elevated, controlled temperature (i.e. the solvent's boiling point) and ambient pressure without losing large quantities of the mixture. [6] The diagram shows a typical reflux apparatus. It includes a water bath to indirectly heat the mixture.
Liebig condenser. The Liebig condenser (/ ˈ l iː b ɪ ɡ /, LEE-big) [1] or straight condenser is a piece of laboratory equipment, specifically a condenser consisting of a straight glass tube surrounded by a water jacket. In typical laboratory operation, such as distillation, the condenser is clamped to a retort stand in vertical
An overhead condenser is a heat exchange equipment used for condensing the mixture leaving the top of the column. Either cooling water or air is used as a cooling agent. An overhead accumulator is a horizontal pressure vessel containing the condensed mixture. Pumps can be used to control the reflux to the column.
A low temperature distillation plant consists of one heat exchanger for the heat transfer from heat source into water and one for the heat transfer from distillate to the re-cooling media. A plant with several cascades has one additional heat exchanger for internal heat recovery (HEX 2) increasing the thermal efficiency of the plant. [ 7 ]
At this pressure, the condensation temperature of the water vapor at the heat exchanger will be 390 K. Taking into account the boiling point elevation of the salt water we wish to evaporate (8 K for a saturated salt solution), this leaves a temperature difference of less than 8 K at the heat exchanger. A small ∆T leads to slow heat transfer ...