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Generally, the maximum safe operating temperature of a mineral oil bath is approximately 160 °C (320 °F), the oil's flash point. Mineral oil cannot be used above 310 °C (590 °F) due to the compound's boiling point. If higher temperatures are needed, a silicone oil or a sand bath may be used instead.
This is achieved using a high-boiling point liquid inside a thermally conducting bath (usually made of metal). Water and silicone oil are the most commonly used fluids. A water bath is used for temperatures up to 100 °C. An oil bath is employed for temperatures over up to and above 100 °C.
A silicone oil is any liquid polymerized siloxane with organic side chains. The most important member is polydimethylsiloxane . These polymers are of commercial interest because of their relatively high thermal stability and their lubricating properties.
The oil level is a little low now to compensate for expansion when heating commences. The Thiele tube, named after the German chemist Johannes Thiele, is a laboratory glassware designed to contain and heat an oil bath. Such a setup is commonly used in the determination of the melting point or boiling point of a substance.
It is also used to enable certain chemical reactions to occur at high temperature. ... alternative methods such as oil bath, silicone oil bath or sand bath may be ...
Note: without the addition of ethylene glycol, temp is -78 °C. Dry ice: Trichloroethylene-73 Dry ice: Isopropyl alcohol-77 Liquid N 2: Butyl acetate-77 Dry ice: Acetone-78 Liquid N 2: Isoamyl acetate-79 Dry ice: Sulfur dioxide-82 Liquid N 2: Ethyl Acetate-84 Liquid N 2: n-Butanol-89 Liquid N 2: Hexane-94 Liquid N 2: Acetone-94 Liquid N 2 ...