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Chloryl tetraperchloratoaurate is produced by the oxidation of gold metal, gold(III) chloride, or chloroauric acid by dichlorine hexoxide: [1] [2] 2 AuCl 3 + 8 Cl 2 O 6 → 2 ClO 2 Au(ClO 4) 4 + 6 ClO 2 + 3 Cl 2. A production of gold(III) perchlorate is attempted by heating this compound, but it instead forms an oxy-perchlorato derivative. [1]
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Au(III) (referred to as the auric) is a common oxidation state, and is illustrated by gold(III) chloride, Au 2 Cl 6. The gold atom centers in Au(III) complexes, like other d 8 compounds, are typically square planar, with chemical bonds that have both covalent and ionic character. Gold(I,III) chloride is also known, an example of a mixed-valence ...
Gold(III) chloride was first prepared in 1666 by Robert Boyle by the reaction of metallic gold and chlorine gas at 180 °C: [1] [6] [7] 2 Au + 3 Cl 2 → Au 2 Cl 6. This method is the most common method of preparing gold(III) chloride. It can also be prepared by reacting gold powder with iodine monochloride: [5] 2 Au + 6 ICl → 2 AuCl 3 + 3 I 2
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