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The method uses headspace gas injected into a gas chromatographic column (GC) to determine the original concentration in a water sample. [9] A sample of water is collected in the field in a vial without headspace and capped with a Teflon septum or crimp top to minimize the escape of volatile gases. It is beneficial to store the bottles upside ...
English: Schematic drawing of the headspace analysis in gas chromatography. After thermal equilibration, a sample is taken out of the headspace and the analytical compounds are seperated and identified on the GC column. Main advantage: Even with complex sample matrices (e.g. blood, honey), the GC column is not contaminated with sample components.
Gas chromatography (GC) is a common type of chromatography used in analytical chemistry for separating and analyzing compounds that can be vaporized without decomposition. Typical uses of GC include testing the purity of a particular substance, or separating the different components of a mixture. [ 1 ]
Analytical thermal desorption, known within the analytical chemistry community simply as "thermal desorption" (TD), is a technique that concentrates volatile organic compounds (VOCs) in gas streams prior to injection into a gas chromatograph (GC). It can be used to lower the detection limits of GC methods, and can improve chromatographic ...
Example of a GC–MS instrument. Gas chromatography–mass spectrometry (GC–MS) is an analytical method that combines the features of gas-chromatography and mass spectrometry to identify different substances within a test sample. [1]
Gas chromatography (GC) in combination with mass spectrometry is capable of separating isomeric compounds. Although GC has been successfully coupled to PTR-MS in the past, [20] this approach annihilates the real-time capability of the PTR-MS technology, because a single GC analysis run typically takes between 30 min and 1 h. Thus, state-of-the ...
Solid-phase microextraction sampling. Solid phase microextraction, or SPME, is a solid phase extraction sampling technique that involves the use of a fiber coated with an extracting phase, that can be a liquid or a solid (), [1] which extracts different kinds of analytes (including both volatile and non-volatile) from different kinds of media, that can be in liquid or gas phase. [2]
Headspace or ullage, the unfilled space in a container; Headspace technology, the gaseous constituents of a closed space above liquids or solid emitting and vapors measured using headspace gas chromatography; Headspace (firearms), a chamber measurement; Headroom (photographic framing), a concept of aesthetic composition in imaging