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The reflux system in a typical industrial distillation column. Reflux is a technique involving the condensation of vapors and the return of this condensate to the system from which it originated. It is used in industrial [1] and laboratory [2] distillations. It is also used in chemistry to supply energy to reactions over a long period of time.
The Marcusson apparatus, Dean-Stark apparatus, Dean–Stark receiver, distilling trap, or Dean–Stark Head is a piece of laboratory glassware used in synthetic chemistry to collect water [1] [2] (or occasionally other liquid) from a reactor. It is used in combination with a reflux condenser and a distillation flask for the separation of water ...
In chemistry, a condenser is laboratory apparatus used to condense vapors – that is, turn them into liquids – by cooling them down. [1] Condensers are routinely used in laboratory operations such as distillation, reflux, and extraction. In distillation, a mixture is heated until the more volatile components boil off, the vapors are ...
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Combining a stack of these gives the system of equations for the whole column. There is a range of solutions, because a higher reflux ratio enables fewer plates, and vice versa. The engineer must then find the optimal solution with respect to acceptable volume holdup, column height and cost of construction.
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This page was last edited on 24 September 2019, at 06:30 (UTC).; Text is available under the Creative Commons Attribution-ShareAlike 4.0 License; additional terms may apply.
Its use has declined due to modern hotplate technology and vacuum pumps. The apparatus was first described in a book edited by Emil Abderhalden. [1] The drying pistol allows the sample to be dried at elevated temperature; this is especially preferred when storage in a desiccator at room temperature does not give satisfactory results. [2]