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Any analyte that can be oxidized or reduced is a candidate for amperometric detection. The simplest form of amperometric detection is single-potential, or direct current (DC), amperometry. A voltage (potential) is applied between two electrodes positioned in the column effluent. The measured current changes as an electroactive analyte is ...
Double-pulsed chronoamperometry waveform showing integrated region for charge determination.. In electrochemistry, chronoamperometry is an analytical technique in which the electric potential of the working electrode is stepped and the resulting current from faradaic processes occurring at the electrode (caused by the potential step) is monitored as a function of time.
Differential pulse voltammetry: An electrochemical technique similar to normal pulse voltammetry but the applied base potential is increased or decreased steadily, and the pulse height: base height ratio is kept constant. In DPV, measurements of current are taken twice during each drop, first immediately before the pulse and second before the ...
The envelope detector has several drawbacks: The input to the detector must be band-pass filtered around the desired signal, or else the detector will simultaneously demodulate several signals. The filtering can be done with a tunable filter or, more practically, a superheterodyne receiver; It is more susceptible to noise than a product detector
Pulse-Height Analyzer Principle: Three pulses, 1, 2, and 3 are detected at different times t. Two discriminators emit a counting signal if their set voltage threshold is exceeded by a pulse. Pulse 2 triggers the Lower Level E L but not the Upper Level E U. Pulse 2 is thus counted into the spectral region denoted as P.
An insulation monitoring device monitors the ungrounded system between an active phase conductor and earth.It is intended to give an alert (light and sound) or disconnect the power supply when the resistance between the two conductors drops below a set value, usually 50 kΩ (sample of IEC standard for medical applications).
Furthermore, in 2009 release of the USP-NF, the United States Pharmacopia made several analyses of ion chromatography available using two techniques: conductivity detection, as well as pulse amperometric detection. Majority of these applications are primarily used for measuring and analyzing residual limits in pharmaceuticals, including ...
Therefore, type I and type II sensors have the same design with gas electrodes combined with metal and an electrolyte where oxidized or reduced ions can be electrochemically equilibrated through the electrochemical cell. In the third type of electrochemical sex, auxiliary phases are added to the electrodes to enhance the selectivity and stability.