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The reflux system in a typical industrial distillation column. Reflux is a technique involving the condensation of vapors and the return of this condensate to the system from which it originated. It is used in industrial [1] and laboratory [2] distillations. It is also used in chemistry to supply energy to reactions over a long period of time.
A liquid (not visible) in the flask at left is heated by the blue mantle to the boiling point. The vapor is then cooled as it goes through the inner tube of the condenser. There it becomes liquid again, and drips into the smaller collecting flask at right, immersed in a cooling bath. The two hoses connected to the condenser circulate water ...
This flask shape is also more resistant to fracturing under vacuum, as a sphere more evenly distributes stress across its surface. Round-bottom flasks are often used to contain chemical reactions run by chemists, especially for reflux set-ups and laboratory-scale synthesis. [3]
A Soxhlet extractor is a piece of laboratory apparatus [1] invented in 1879 by Franz von Soxhlet. [2] It was originally designed for the extraction of a lipid from a solid material. Typically, Soxhlet extraction is used when the desired compound has a limited solubility in a solvent, and the impurity is insoluble in that solvent. It allows for ...
The Marcusson apparatus, Dean-Stark apparatus, Dean–Stark receiver, distilling trap, or Dean–Stark Head is a piece of laboratory glassware used in synthetic chemistry to collect water [1] [2] (or occasionally other liquid) from a reactor. It is used in combination with a reflux condenser and a distillation flask for the separation of water ...
Büchner flask or sidearm flask—a thick-walled conical flask with a short hose-connection tube on the side of the neck. Volumetric flask —for preparing liquids with volumes of high precision. It is a flask with an approximately pear-shaped body and a long neck with a circumferential fill line.