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Fourier transform infrared spectroscopy (FTIR) [1] is a technique used to obtain an infrared spectrum of absorption or emission of a solid, liquid, or gas. An FTIR spectrometer simultaneously collects high-resolution spectral data over a wide spectral range.
Reflection-absorption FTIR: Sample is usually prepared as a thick block and is polished into a smooth surface. [4] As the IR beam strikes the sample surface, some of the energy is absorbed by the top layer (<10 μm) of the bulk sample. The altered incident beam is then reflected and carry the composition information of the targeted surface area.
In all three spectroscopic methods, the sample usually needs to be present in solution, which may present problems during forensic examination because it necessarily involves sampling solid from the object to be examined. In FTIR, three types of samples can be analyzed: solution , powder, or film. A solid film is the easiest and most straight ...
multiple broad peaks C─O alcohols: primary 1040–1060 strong, broad secondary ~1100 strong tertiary 1150–1200 medium phenols any 1200 ethers aliphatic 1120 aromatic 1220–1260 carboxylic acids any 1250–1300 esters any 1100–1300 two bands (distinct from ketones, which do not possess a C─O bond) C─N aliphatic amines any 1020–1220
The peak at the center is the ZPD position ("zero path difference"): Here, all the light passes through the interferometer because its two arms have equal length. The method of Fourier-transform spectroscopy can also be used for absorption spectroscopy. The primary example is "FTIR Spectroscopy", a common technique in chemistry.
The sample, liquid or solid, is placed into the sample cup which is inserted into the photoacoustic cell which is then sealed for the measurement. The sample may be one solid piece, powder or basically in any form for the measurement. For example, a piece of rock can be inserted into the sample cup and the spectrum measured from it. [citation ...
The linear absorption (FTIR) spectrum is indicated above the 2D IR spectrum. The two peaks in the 1D spectrum reveal no information on coupling between the two states. After the waiting time in the experiment, it is possible to reach double excited states. This results in the appearance of an overtone peak.
nano-FTIR absorption and far-field FTIR (ATR modality) spectra measured on the same polymer sample show great agreement. Placement of the sample stage into one of the interferometer's arms (instead of outside of the interferometer as typically implemented in conventional FTIR ) is a key element of nano-FTIR.