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Cut glass wine glass made of lead glass. Lead glass, commonly called crystal, is a variety of glass in which lead replaces the calcium content of a typical potash glass. [1] Lead glass contains typically 18–40% (by mass) lead(II) oxide (PbO), while modern lead crystal, historically also known as flint glass due to the original silica source, contains a minimum of 24% PbO. [2]
Stiegel's works was the first to make lead glass in America. [50] The lead glass of this time period, commonly known as crystal because it was colorless and transparent, was typically used for fine tableware. [51] According to the American Philosophical Society, Stiegel's lead glass was "equal in beauty and quality to the generality of Flint ...
There is a relatively large difference in the electronegativity of lead(II) at 1.87 and lead(IV) at 2.33. This difference marks the reversal in the trend of increasing stability of the +4 oxidation state going down the carbon group; tin, by comparison, has values of 1.80 in the +2 oxidation state and 1.96 in the +4 state. [63]
Stiegel's glass works in the Province of Pennsylvania was the first in America to make fine lead crystal, which is often mislabeled as flint glass. [64] Amelung invested more money in glassmaking than anyone ever had and produced impressive quality glass with engraving—although his Maryland glass works failed after 11 years. [65]
2 Pb(NO 3) 2 → 2 PbO + 4 NO 2 + O 2 PbCO 3 → PbO + CO 2. PbO is produced on a large scale as an intermediate product in refining raw lead ores into metallic lead. The usual lead ore is galena (lead(II) sulfide). At a temperature of around 1,000 °C (1,800 °F) in air, the sulfide converted to the oxide: [4] 2 PbS + 2 O 2 → 2 PbO + 2 SO 2
Crystal glass (sometimes called flint glass) is a high-quality clear glass that needs an additive known as red lead. In the British colonies that would become the United States, crystal began being produced right before 1770 by a works led by Henry William Stiegel in the Province of Pennsylvania . [ 23 ]
Lead was used for roof covering material and water supply and waste pipes. The Latin name for lead is plumbum, thus plumbing. Romans also made use of glass in construction with colored glass in mosaics and clear glass for windows. Glass came to be fairly commonly used in windows of public buildings. [2]
Lead oxide is the traditional low temperature flux used for crystal glass, but it is now avoided because it is toxic even in small quantities. It is being replaced by other substances, especially boron and zinc oxides. [3] In clay bodies a flux creates a limited and controlled amount of glass, which works to cement crystalline phases together.