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Synthesis of DDQ involves cyanation of chloranil. J. Thiele and F. Günther first reported a 6-step preparation in 1906. [7] The substance did not receive interest until its potential as a dehydrogenation agent was discovered. A single-step chlorination from 2,3-dicyanohydroquinone was reported in 1965. [8]
The use of protective groups is pervasive but not without criticism. [103] In practical terms their use adds two steps (protection-deprotection sequence) to a synthesis, either or both of which can dramatically lower chemical yield. Crucially, added complexity impedes the use of synthetic total synthesis in drug discovery.
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The Journal of Emerging Market Finance [1] is a triannual peer-reviewed academic journal covering the theory and practice of finance in emerging markets. The journal was established in 2002 and is published tri-annually by SAGE Publications. The editor-in-chief is G. Balasubramanian [2] (Institute for Financial Management and Research).
The use of triethylsilane as a carbocation scavenger in the presence of trifluoroacetic acid in dichloromethane has been shown to lead to increased yields, decreased reaction times, simple work-up and improved selectivity for the deprotection of t-butyl ester and t-butoxycarbonyl sites in protected amino-acids and peptides in the presence of ...
In northern Peru, the World Bank's business-lending arm is part owner of the Yanacocha gold mine, accused by impoverished farming communities of despoiling their land in pursuit of the precious ore. The bank and IFC have stepped up investments in projects deemed to have a high risk of serious and environment damage, including oil pipelines, mines and even coal-fired power plants, an ...
According to its first editor, Michael R. Darby, the journal was established to cope with the explosive growth of research on international finance.In its focus on this field, the journal used a broad definition encompassing, among others, topics such as optimum currency area, international financial institutions, open economy macroeconomics, and international asset pricing models.
The first reported use of a PPG in the scientific literature was by Barltrop and Schofield, who in 1962 used 253.7 nm light to release glycine from N-benzylglycine. [4] Following this initial report, the field rapidly expanded throughout the 1970s as Kaplan [6] and Epstein [7] studied PPGs in a variety of biochemical systems. During this time ...