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The geometry of the still also plays a role in determining how much reflux occurs. In a pot still, if the tube leading from the boiler to the condenser, the lyne arm, is angled upward, more liquid will have a chance to condense and flow back into the boiler leading to increased reflux. Typical results can increase production as high as 50% over ...
As in the tube condenser, the heat of condensation is carried away by natural convection. Any vapor that does not condense in the head may still condense in the neck. Still head type condensers are now rarely used in laboratories, and are usually topped by some other type of reflux condenser where most of the condensation takes place.
Examples include the Liebig condenser, Graham condenser, and Allihn condenser. This is not to be confused with a condensation reaction which links two fragments into a single molecule by an addition reaction and an elimination reaction. In laboratory distillation, reflux, and rotary evaporators, several types of condensers are commonly used ...
The solvent is heated to reflux. The solvent vapour travels up a distillation arm, and floods into the chamber housing the thimble of solid. The condenser ensures that any solvent vapour cools, and drips back down into the chamber housing the solid material. The chamber containing the solid material slowly fills with warm solvent.
It is used in combination with a reflux condenser and a distillation flask for the separation of water from liquids. This may be a continuous removal of the water that is produced during a chemical reaction performed at reflux temperature, such as in esterification reactions. The original setup by Julius Marcusson (invented in 1905) was refined ...
Liebig condenser. The Liebig condenser (/ ˈ l iː b ɪ ɡ /, LEE-big) [1] or straight condenser is a piece of laboratory equipment, specifically a condenser consisting of a straight glass tube surrounded by a water jacket. In typical laboratory operation, such as distillation, the condenser is clamped to a retort stand in vertical