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Ammonium phosphomolybdate can be made by heating ammonium orthomolybdate combined with phosphoric acid and nitric acid, yielding ammonium nitrate, water, and a yellow precipitate of ammonium phosphomolybdate is obtained. [3] 12 (NH 4) 6 Mo 7 O 24 (H 2 O) 4 + 7 Na 2 HPO 4 (H 2 O) + 65 HNO 3 → 7 (NH 4) 3 Mo 12 PO 40 + 51 NH 4 NO 3 + 14 NaNO 3 ...
A simple qualitative method to determine the presence of phosphate ions in a sample is as follows. A small amount of the sample is acidified with concentrated nitric acid, to which a little ammonium molybdate is added. The presence of phosphate ions is indicated by the formation of a bright yellow precipitate layer of ammonium phosphomolybdate ...
Ammonium heptamolybdate is the inorganic compound whose chemical formula is (NH 4) 6 Mo 7 O 24, normally encountered as the tetrahydrate.A dihydrate is also known. It is a colorless solid, often referred to as ammonium paramolybdate or simply as ammonium molybdate, although "ammonium molybdate" can also refer to ammonium orthomolybdate, (NH 4) 2 MoO 4, and several other compounds.
In chemistry, a molybdate is a compound containing an oxyanion with molybdenum in its highest oxidation state of +6: O − −Mo(=O) 2 −O −. Molybdenum can form a very large range of such oxyanions , which can be discrete structures or polymeric extended structures, although the latter are only found in the solid state.
The molybdovanadate reagent is a solution containing both the molybdate and vanadate ions. It is commonly used in the determination of phosphate ion content. [1] [2] The reagent used is ammonium molybdovanadate with the addition of 70% perchloric acid (sulfuric acid is also known to be used).
Ammonium orthomolybdate is the inorganic compound with the chemical formula (NH 4) 2 MoO 4. It is a white solid that is prepared by treating molybdenum trioxide with aqueous ammonia. Upon heating these solutions, ammonia is lost, to give ammonium heptamolybdate ((NH 4 ) 6 Mo 7 O 24 ·4H 2 O).
Ammonium dimolybdate (ADM) is the inorganic compound with the formula (NH 4) 2 Mo 2 O 7. It is a white, water-soluble solid. ADM is an intermediate in the production of molybdenum compounds from its ores. Roasting typical ore produces crude molybdenum(VI) oxides, which can be extracted into aqueous ammonia, affording ammonium molybdate. Heating ...
The United States Department of Justice method for producing the reagent is the addition of 100 ml of hot, concentrated (95–98%) sulfuric acid to 0.5 g of sodium molybdate or molybdic acid. [1] The Virginia Department of Forensic Science method uses 0.5 g ammonium molybdate per 100 ml H 2 SO 4 (conc.) [2]