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Organic solvent extraction is the most common and most economically important technique for extracting aromatics in the modern perfume industry. Raw materials are submerged and agitated in a solvent that can dissolve the desired aromatic compounds. Commonly used solvents for maceration/solvent extraction include hexane, and dimethyl ether.
First, plant material is extracted with a hydrocarbon solvent, such as hexane, to yield concrete. The concrete is then extracted with ethanol. The ethanol extract is cooled (e.g., to −15 °C) to solidify waxes, and cold filtered to yield a liquid extract. When the ethanol evaporates, an oil—the absolute—is left behind. [1]
Rose is one of the most popular natural flowers used in perfumery. A semi-solid residue of essential oils, waxes, resins and other oil-soluble plant chemicals remains. [2] The solvent used for extraction must be chosen carefully regarding its polarity and boiling point. If the boiling point is too high, compounds that are readily deactivated by ...
In modern vegetable oil production, oils are usually extracted chemically, using a solvent such as hexane. Chemical extraction is cheaper and more efficient than mechanical extraction, at a large scale, leaving only 0.5–0.7% of the oil in the plant solids, as compared to 6–14% for mechanical extraction. [4]
In the solvent extraction method, the flowers are agitated in a vat with a solvent such as hexane, which draws out the aroma compounds as well as other soluble substances such as wax and pigments. The extract is subjected to vacuum processing which removes the solvent for re-use. The remaining waxy mass is known as a concrete.
The enfleurage fragrance extraction method is one of the oldest. It is also highly inefficient and costly but was the sole method of extracting the fragrant compounds in delicate flowers such as jasmine and tuberose, which would be destroyed or denatured by the high temperatures required by methods of fragrance extraction such as steam distillation.