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Gold(III) chloride was first prepared in 1666 by Robert Boyle by the reaction of metallic gold and chlorine gas at 180 °C: [1] [6] [7] 2 Au + 3 Cl 2 → Au 2 Cl 6. This method is the most common method of preparing gold(III) chloride. It can also be prepared by reacting gold powder with iodine monochloride: [5] 2 Au + 6 ICl → 2 AuCl 3 + 3 I 2
Gold(I,III) chloride (gold dichloride, tetragold octachloride), Au 4 Cl 8 Gold(III) chloride (gold trichloride, digold hexachloride), Au 2 Cl 6 Chloroauric acid , HAuCl 4 (brown gold chloride); or its sodium salt, sodium tetrachloroaurate , NaAuCl 4 (gold chloride, sodium gold chloride, yellow gold chloride), used as a histological stain
Single crystals of gold(I,III) chloride are triclinic with a P 1 space group and consist of discrete Au 4 Cl 8 molecules with idealised C 2h symmetry. [1] Within this the Au(I) centers are linearly coordinated with a Cl-Au-Cl bond angle of 175.0° (close to the ideal value of 180°) and an average bond length of 2.30 Å.
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At still higher temperatures, around 500 °C, all gold chlorides convert to gold. This conversion is key to the Miller process, which is widely used for the purification of gold. [2] Reaction with potassium bromide yields potassium auric bromide and potassium chloride with separation of metallic gold: 3 AuCl + 4 KBr → KAuBr 4 + 2 Au + 3 KCl
In chemistry, hypochlorite, or chloroxide is an anion with the chemical formula ClO −.It combines with a number of cations to form hypochlorite salts. Common examples include sodium hypochlorite (household bleach) and calcium hypochlorite (a component of bleaching powder, swimming pool "chlorine"). [1]