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A Karl Fischer titrator. In analytical chemistry, Karl Fischer titration is a classic titration method that uses coulometric or volumetric titration to determine trace amounts of water in a sample. It was invented in 1935 by the German chemist Karl Fischer. [1] [2] Today, the titration is done with an automated Karl Fischer titrator.
Karl Fischer (24 March 1901 – 16 April 1958) was a German chemist. [1] In 1935 he published a method to determine trace amounts of water in samples. [2] This method is now called Karl Fischer titration and was originally performed manually but has been automated. It remains the primary method of water content determination used worldwide by ...
Karl Fischer Coulometer Auto Titrator. The Karl Fischer reaction uses a coulometric titration to determine the amount of water in a sample. It can determine concentrations of water on the order of milligrams per liter. It is used to find the amount of water in substances such as butter, sugar, cheese, paper, and petroleum.
Food moisture analysis is the determination of the concentration of water in a food sample. A variety of techniques may be used including Karl Fischer titration and loss on drying. Many technical standards exist which define test methods for determining moisture in different types of food.
Moisture dew point is the temperature at which moisture condenses out of a gas. This parameter is inherently related to the moisture content, which defines the amount of water molecules as a fraction of the total. Both can be used as a measure of the amount of moisture in a gas and one can be calculated from the other fairly accurately.
A sample is dissolved in methanol, and titrated with Karl Fischer reagent (consists of iodine, sulfur dioxide, a base and a solvent, such as alcohol). The reagent contains iodine, which reacts proportionally with water. Thus, the water content can be determined by monitoring the electric potential of excess iodine. [52]
Water content or moisture content is the quantity of water contained in a material, such as soil (called soil moisture), rock, ceramics, crops, or wood. Water content is used in a wide range of scientific and technical areas, and is expressed as a ratio, which can range from 0 (completely dry) to the value of the materials' porosity at saturation.
moisture (Karl Fischer titration) Wet chemistry is also used in environmental chemistry settings to determine the current state of the environment. It is used to test: [citation needed] Biochemical Oxygen Demand (BOD) Chemical Oxygen Demand (COD) eutrophication; coating identification