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In rotary evaporation a vacuum distillation apparatus is used to remove bulk solvents from a sample. Typically the vacuum is generated by a water aspirator or a membrane pump. In a Kugelrohr apparatus a short path distillation apparatus is typically used (generally in combination with a (high) vacuum) to distill high boiling (> 300 °C ...
The fractional distillation of organic substances played an important role in the 9th-century works attributed to the Islamic alchemist Jabir ibn Hayyan, as for example in the Kitāb al-Sabʿīn ('The Book of Seventy'), translated into Latin by Gerard of Cremona (c. 1114–1187) under the title Liber de septuaginta. [1]
A still is an apparatus used to distill liquid mixtures by heating to selectively boil and then cooling to condense the vapor. [1] A still uses the same concepts as a basic distillation apparatus, but on a much larger scale.
A simple short path vacuum distillation apparatus can be used for bulb-to-bulb distillation. 1: Still pot with stirrer bar/anti-bumping granules 2: Cold finger - Condenser with maximum surface to condense most of the vapour. 3: Cooling water outlet 4: cooling water inlet 5: Vacuum Adapter 6: Receiving Flask.
Modern vessels now use flash-type evaporators to boil seawater, heating the water to between 70 and 80 °C (158 and 176 °F) and evaporating the water in a vacuum; this is then collected as condensation before being stored. Solar stills can be relatively simple to design and build, with very cheap materials. [12]
Solar is still affordable, eco-friendly, and considered an effective method amongst other conventional distillation techniques. Solar still is very effective, especially for supplying fresh water for islanders. This makes them ideal for use in rural areas or developing countries where access to clean water is limited. [12] [13]
Short-path distillation is a distillation technique that involves the distillate traveling a short distance, often only a few centimeters, and is normally done at reduced pressure. [ 1 ] [ 2 ] Short-path distillation systems often have a variety of names depending on the manufacturer of the system and what compounds are being distilled within them.
A simple vacuum distillation system can be used, whereby the vacuum is replaced with an inert gas after the distillation is complete. However, this is a less satisfactory system if one desires to collect fractions under a reduced pressure.