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Differential scanning calorimetry (DSC) is a thermoanalytical technique in which the difference in the amount of heat required to increase the temperature of a sample and reference is measured as a function of temperature. [1] Both the sample and reference are maintained at nearly the same temperature throughout the experiment.
Characteristic DSC curve for a polyethylene, the OIT is measured. Oxidation induction time or OIT is a standardized test performed in a DSC which measures the level of thermal stabilization of the material tested. The time between melting and the onset of decomposition in isothermal conditions is measured.
In a differential scanning calorimeter (DSC), heat flow into a sample—usually contained in a small aluminium capsule or 'pan'—is measured differentially, i.e., by comparing it to the flow into an empty reference pan. In a heat flux DSC, both pans sit on a small slab of material with a known (calibrated) heat resistance K. The temperature of ...
By coupling the thermal analysis instrument, e. g. TGA (thermogravimetry) or DSC (differential scanning calorimetry), with a fast Quadrupole Mass Spectrometer (QMS) the detection of gas separation and identification of the separated components are possible in exact time correlation with the other thermal analysis signals. DSC/TGA-QMS or TGA-QMS ...
Polymers represent another large area in which thermal analysis finds strong applications. Thermoplastic polymers are commonly found in everyday packaging and household items, but for the analysis of the raw materials, effects of the many additive used (including stabilisers and colours) and fine-tuning of the moulding or extrusion processing used can be achieved by using differential scanning ...
An example of a Co-Flux Calorimeter. Constant flux calorimetry is an advanced temperature control mechanism used to generate accurate calorimetry. It operates by controlling the jacket area of a laboratory reactor while maintaining a constant inlet temperature of the thermal fluid. This method allows for precise temperature control, even during ...
Download as PDF; Printable version; ... Chemical formula. C 7 H 14 N 2: Molar mass: ... Thermal hazard analysis by differential scanning calorimetry (DSC) ...
This article presents a set of useful conversions and formulas for air dispersion modeling of atmospheric pollutants and for complying with the various regulations as to how to express the concentrations obtained by such modeling.