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A vacuum tight seal and stability of the Büchner flask and filter are essential during the filtration process. A Büchner ring can be used with Büchner funnels, flasks, glass crucibles and Gooch crucibles. The wide flange and large surface contact ensures an excellent vacuum tight seal whilst the rings are easy to remove and offer excellent ...
The inert-gas line is vented through an oil bubbler, while solvent vapors and gaseous reaction products are prevented from contaminating the vacuum pump by a liquid-nitrogen or dry-ice/acetone cold trap. Special stopcocks or Teflon taps allow vacuum or inert gas to be selected without the need for placing the sample on a separate line. [3]
Filtration is a unit operation that is commonly used both in laboratory and production conditions. This apparatus, adapted for laboratory work, is often used to isolate the product of synthesis of a reaction when the product is a solid in suspension. The product of synthesis is then recovered faster, and the solid is drier than in the case of a ...
In the field of oil regeneration and re-refining, vacuum pumps create a low vacuum for oil dehydration and a high vacuum for oil purification. [44] A vacuum may be used to power, or provide assistance to mechanical devices. In hybrid and diesel engine motor vehicles, a pump fitted on the engine (usually on the camshaft) is used to produce a vacuum.
Cross section of a Büchner Flask. Note the hose barb pointing right for attaching a vacuum source. A Büchner flask, also known as a vacuum flask, [1] filter flask, suction flask, side-arm flask, or Bunsen flask, is a thick-walled Erlenmeyer flask with a short glass tube and hose barb protruding about an inch from its neck.
The sorption pump is a vacuum pump that creates a vacuum by adsorbing molecules on a very porous material like molecular sieve which is cooled by a cryogen, typically liquid nitrogen. The ultimate pressure is about 10 −2 mbar. With special techniques this can be lowered till 10 −7 mbar.
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