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Sample preparation for mass spectrometry is used for the optimization of a sample for analysis in a mass spectrometer (MS). Each ionization method has certain factors that must be considered for that method to be successful, such as volume, concentration, sample phase, and composition of the analyte solution. Quite possibly the most important ...
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Standard solutions are generally prepared by dissolving a solute of known mass into a solvent to a precise volume, or by diluting a solution of known concentration with more solvent. [1] A standard solution ideally has a high degree of purity and is stable enough that the concentration can be accurately measured after a long shelf time. [2]
A mass chromatogram is a representation of mass spectrometry data as a chromatogram, where the x-axis represents time and the y-axis represents signal intensity. [1] The source data contains mass information; however, it is not graphically represented in a mass chromatogram in favor of visualizing signal intensity versus time.
For example, the ionic strength of the solution can have an effect on the activity coefficients of the analytes. [3] [4] The most common approach for accounting for matrix effects is to build a calibration curve using standard samples with known analyte concentration and which try to approximate the matrix of the sample as much as possible. [2]
Gas chromatography–mass spectrometry (GC–MS) is an analytical method that combines the features of gas-chromatography and mass spectrometry to identify different substances within a test sample. [1] Applications of GC–MS include drug detection, fire investigation, environmental analysis, explosives investigation, food and flavor analysis ...
One of the most widely used methods for headspace analysis is described by the United States Environmental Protection Agency (USEPA). Originally developed by the R.S. Kerr USEPA Laboratory in Ada, Oklahoma as a "high quality, defendable, and documented way to measure" methane, ethane, and ethene, [7] [8] RSKSOP-175 is a standard operating procedure (SOP) and an unofficial method employed by ...
Suppose there are known concentrations of nickel in a set of calibration solutions: 0 ppm, 1.6 ppm, 3.2 ppm, 4.8 ppm, 6.4 ppm, and 8 ppm. Each solution also has 5 ppm yttrium to act as an internal standard. If these solutions are measured using ICP-OES, the intensity of the yttrium signal should be consistent across all solutions.