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The percent crystalline content of a polymer can be estimated from the crystallization/melting peaks of the DSC graph using reference heats of fusion found in the literature. [25] DSC can also be used to study thermal degradation of polymers using an approach such as Oxidative Onset Temperature/Time (OOT); however, the user risks contamination ...
Differential thermal analysis (DTA) is a thermoanalytic technique that is similar to differential scanning calorimetry. In DTA, the material under study and an inert reference are made to undergo identical thermal cycles, (i.e., same cooling or heating programme) while recording any temperature difference between sample and reference. [ 1 ]
These first Heisler–Gröber charts were based upon the first term of the exact Fourier series solution for an infinite plane wall: (,) = = [ + ], [1]where T i is the initial uniform temperature of the slab, T ∞ is the constant environmental temperature imposed at the boundary, x is the location in the plane wall, λ is the root of λ * tan λ = Bi, and α is thermal diffusivity.
Polymers represent another large area in which thermal analysis finds strong applications. Thermoplastic polymers are commonly found in everyday packaging and household items, but for the analysis of the raw materials, effects of the many additive used (including stabilisers and colours) and fine-tuning of the moulding or extrusion processing used can be achieved by using differential scanning ...
In fracture mechanics, the energy release rate, , is the rate at which energy is transformed as a material undergoes fracture.Mathematically, the energy release rate is expressed as the decrease in total potential energy per increase in fracture surface area, [1] [2] and is thus expressed in terms of energy per unit area.
x is displacement; E(x) is energy; Q is the heat of adsorption or binding energy; a is the spacing between adjacent adsorption sites; E diff is the barrier to diffusion. Surface diffusion kinetics can be thought of in terms of adatoms residing at adsorption sites on a 2D lattice , moving between adjacent (nearest-neighbor) adsorption sites by a ...
Chilton–Colburn J-factor analogy (also known as the modified Reynolds analogy [1]) is a successful and widely used analogy between heat, momentum, and mass transfer.The basic mechanisms and mathematics of heat, mass, and momentum transport are essentially the same.
In condensed matter physics and crystallography, the static structure factor (or structure factor for short) is a mathematical description of how a material scatters incident radiation. The structure factor is a critical tool in the interpretation of scattering patterns ( interference patterns ) obtained in X-ray , electron and neutron ...