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Common gases that produce negative air ions include single-component gases such as nitrogen, oxygen, carbon dioxide, water vapor, or multi-component gases obtained by mixing these single-component gases. Various negative air ions are formed by combining active neutral molecules and electrons in the gas through a series of ion-molecule reactions ...
In many mass spectrometry ionization methods, the sample must be in the liquid or gas phase for the ionization method to work. Sample preparation to ensure proper ionization can be difficult, but can be made easier by coupling the mass spectrometer to some chromatographic equipment.
Many mass spectrometers work in either negative ion mode or positive ion mode. It is very important to know whether the observed ions are negatively or positively charged. This is often important in determining the neutral mass but it also indicates something about the nature of the molecules.
The nitrogen bonds to the surface metals and has electro-negative properties that help exclude unwanted ions and molecules, while phosphate, sulfate, nitrate and hydroxyl surface ions block chlorine and prevent corrosion. 10 mA/cm 2 can be achieved using 1.52 and 1.55 V in alkaline electrolyte and seawater, respectively.
Reagent gas molecules (often methane or ammonia) [4] are ionized by electron ionization to form reagent ions, which subsequently react with analyte molecules in the gas phase to create analyte ions for analysis by mass spectrometry. Negative chemical ionization (NCI), charge-exchange chemical ionization, atmospheric-pressure chemical ionization ...
The ions generated from atmospheric or dopant molecules undergo ion-molecule reactions with the sample molecules to produce analyte ions. Analytes with low ionization energy may be ionized directly. The DART ionization process can produce positive or negative ions depending on the potential applied to the exit electrode.
Atmospheric pressure chemical ionization chamber cross section. Atmospheric pressure chemical ionization (APCI) is an ionization method used in mass spectrometry which utilizes gas-phase ion-molecule reactions at atmospheric pressure (10 5 Pa), [1] [2] commonly coupled with high-performance liquid chromatography (HPLC). [3]
Atmospheric pressure photoionization (APPI) is a soft ionization method used in mass spectrometry (MS) usually coupled to liquid chromatography (LC). Molecules are ionized using a vacuum ultraviolet (VUV) light source operating at atmospheric pressure (105 Pa), either by direct absorption followed by electron ejection or through ionization of a ...