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A fractionating column or fractional column is equipment used in the distillation of liquid mixtures to separate the mixture into its component parts, or fractions, based on their differences in volatility. Fractionating columns are used in small-scale laboratory distillations as well as large-scale industrial distillations.
The apparatus is assembled as in the diagram. (The diagram represents a batch apparatus as opposed to a continuous apparatus.) The mixture is put into the round-bottomed flask along with a few anti-bumping granules (or a Teflon-coated magnetic stirrer bar if using magnetic stirring), and the fractionating column is fitted into the top. The ...
The typical McCabe–Thiele diagram in Figure 1 uses a q-line representing a partially vaporized feed. Example q-line slopes are presented in Figure 2. The number of steps between the operating lines and the equilibrium line represents the number of theoretical plates (or equilibrium stages) required for the distillation.
Therefore, fractional distillation must be used to separate the components by repeated vaporization-condensation cycles within a packed fractionating column. This separation, by successive distillations, is also referred to as rectification. [41] As the solution to be purified is heated, its vapors rise to the fractionating column. As it rises ...
Fractionation makes it possible to isolate more than two components in a mixture in a single run. This property sets it apart from other separation techniques. Fractionation is widely employed in many branches of science and technology. Mixtures of liquids and gasses are separated by fractional distillation by difference in boiling point.
This image is a derivative work of the following images: Image:Fractional_distillation_lab_apparatus.png licensed with GFDL-en . 2008-03-07T11:17:34Z VIGNERON 272x321 (3971 Bytes) {{GFDL-with-disclaimers}} {{Information |Description=Diagram , drawn by theresa knott.
The apparatus shown in the diagram represents a batch distillation as opposed to a continuous distillation. The liquid feed mixture to be distilled is placed into the round-bottomed flask along with a few anti-bumping granules, and the fractionating column is fitted into the top. As the mixture is heated and boils, vapor rises up the column.
Laboratory distillation set-up using, without a fractionating column 1: Heat source 2: Still pot 3: Still head 4: Thermometer/Boiling point temperature 5: Condenser 6: Cooling water in 7: Cooling water out 8: Distillate/receiving flask 9: Vacuum/gas inlet 10: Still receiver 11: Heat control 12: Stirrer speed control 13: Stirrer/heat plate