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The thermal conductivity detector (TCD), also known as a katharometer, is a bulk property detector and a chemical specific detector commonly used in gas chromatography. [1] This detector senses changes in the thermal conductivity of the column eluent and compares it to a reference flow of carrier gas. Since most compounds have a thermal ...
There are a number of possible ways to measure thermal conductivity, each of them suitable for a limited range of materials, depending on the thermal properties and the medium temperature. Three classes of methods exist to measure the thermal conductivity of a sample: steady-state, time-domain, and frequency-domain methods.
The transient hot wire method has advantage over the other thermal conductivity methods, since there is a fully developed theory and there is no calibration or single-point calibration. Furthermore, because of the very small measuring time (1 s) there is no convection present in the measurements and only the thermal conductivity of the fluid is ...
The main advantages of the 3ω-method are minimization of radiation effects and easier acquisition of the temperature dependence of the thermal conductivity than in the steady-state techniques. Although some expertise in thin film patterning and microlithography is required, this technique is considered as the best pseudo-contact method available.
The measured signal from the thermal conductivity detector for the unknown sample can then be converted into a nitrogen content. As with the Kjeldahl method , conversion of the concentration of nitrogen in a sample to the crude protein content is performed using conversion factors which depend on the particular amino acid sequence of the ...
The technique is widely used across a range of applications, both as a routine quality test and as a research tool. The equipment is easy to calibrate, using low melting indium at 156.5985 °C for example, and is a rapid and reliable method of thermal analysis. [citation needed]
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