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Reflection-absorption FTIR: Sample is usually prepared as a thick block and is polished into a smooth surface. [4] As the IR beam strikes the sample surface, some of the energy is absorbed by the top layer (<10 μm) of the bulk sample. The altered incident beam is then reflected and carry the composition information of the targeted surface area.
Fourier transform infrared spectroscopy (FTIR) [1] is a technique used to obtain an infrared spectrum of absorption or emission of a solid, liquid, or gas. An FTIR spectrometer simultaneously collects high-resolution spectral data over a wide spectral range.
multiple broad peaks C─O alcohols: primary 1040–1060 strong, broad secondary ~1100 strong tertiary 1150–1200 medium phenols any 1200 ethers aliphatic 1120 aromatic 1220–1260 carboxylic acids any 1250–1300 esters any 1100–1300 two bands (distinct from ketones, which do not possess a C─O bond) C─N aliphatic amines any 1020–1220
The peak at the center is the ZPD position ("zero path difference"): Here, all the light passes through the interferometer because its two arms have equal length. The method of Fourier-transform spectroscopy can also be used for absorption spectroscopy. The primary example is "FTIR Spectroscopy", a common technique in chemistry.
It is also used in forensic analysis in both criminal and civil cases, for example in identifying polymer degradation. It can be used in determining the blood alcohol content of a suspected drunk driver. IR spectroscopy has been used in identification of pigments in paintings [2] and other art objects [3] such as illuminated manuscripts. [4]
The linear absorption (FTIR) spectrum is indicated above the 2D IR spectrum. The two peaks in the 1D spectrum reveal no information on coupling between the two states. After the waiting time in the experiment, it is possible to reach double excited states. This results in the appearance of an overtone peak.
A common spectroscopic method for analysis is Fourier transform infrared spectroscopy (FTIR), where chemical bonds can be detected through their characteristic infrared absorption frequencies or wavelengths. These absorption characteristics make infrared analyzers an invaluable tool in geoscience, environmental science, and atmospheric science.
The spectra are plotted in units of log inverse reflectance (log 1/R) versus wavenumber. Alternative plots of Kubelka-Munk units can be used, which relate reflectance to concentration using a scaling factor. A reflectance standard is needed in order to quantify the reflectance of the sample because it cannot be determined directly. [2] [3]