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X-ray absorption spectroscopy (XAS) is a widely used technique for determining the local geometric and/or electronic structure of matter. [1] The experiment is usually performed at synchrotron radiation facilities, which provide intense and tunable X-ray beams. Samples can be in the gas phase, solutions, or solids. [2]
When the incident x-ray energy matches the binding energy of an electron of an atom within the sample, the number of x-rays absorbed by the sample increases dramatically, causing a drop in the transmitted x-ray intensity. This results in an absorption edge.
X-ray microscopes work by exposing a film or charged coupled device detector to detect X-rays that pass through the specimen. The image formed is of a thin section of specimen. Newer X-ray microscopes use X-ray absorption spectroscopy to heterogeneous materials at high spatial resolution. The essence of the technique is a combination of ...
X-ray absorption near edge structure (XANES), also known as near edge X-ray absorption fine structure (NEXAFS), is a type of absorption spectroscopy that indicates the features in the X-ray absorption spectra of condensed matter due to the photoabsorption cross section for electronic transitions from an atomic core level to final states in the energy region of 50–100 eV above the selected ...
There exist several efficient designs for analyzing an X-ray emission spectrum in the ultra soft X-ray region. The figure of merit for such instruments is the spectral throughput, i.e. the product of detected intensity and spectral resolving power. Usually, it is possible to change these parameters within a certain range while keeping their ...
The XANES energy region [3] extends between the edge region and the EXAFS region over a 50-100 eV energy range around the core level x-ray absorption threshold. Before 1980 the XANES region was wrongly assigned to different final states: a) unoccupied total density of states, or b) unoccupied molecular orbitals (kossel structure) or c) unoccupied atomic orbitals or d) low energy EXAFS ...
PIRX (previously XAS) is a bending-magnet-based beamline dedicated to microscopy and spectroscopy in the soft X-ray energy range.The beamline is designed to study chemical and electronic, structural and magnetic properties by means of X-ray absorption spectroscopy (XAS), X-ray natural linear dichroism (XNLD) and X-ray magnetic circular dichroism (XMCD), X-ray magnetic linear dichroism (XMLD ...
RIXS is bulk sensitive: the penetration depth of resonant X-ray photons depends on the material and on the scattering geometry, but typically is of the order of a few micrometers in the hard X-rays regime (for example at transition metal K-edges) and on the order of 0.1 micrometers in the soft X-ray regime (e.g. transition metal L-edges). [1 ...