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2-Bromoanisole is an organobromide with the formula BrC 6 H 4 OCH 3. A colorless liquid, it is one of three isomers of bromoanisole, the others being 3-bromoanisole and 4-bromoanisole . It is a standard coupling partner in metal catalyzed coupling reactions.
CH 3 OC 6 H 5 + (CH 3 CO) 2 O → CH 3 OC 6 H 4 C(O)CH 3 + CH 3 CO 2 H. Unlike most acetophenones, but reflecting the influence of the methoxy group, methoxyacetophenone undergoes a second acetylation. Many related reactions have been demonstrated. For example, phosphorus pentasulfide (P 4 S 10) converts anisole to Lawesson's reagent, [(CH 3 OC ...
4-Bromoanisole is the organobromine compound with the formula CH 3 OC 6 H 4 Br. It is colorless liquid with a pleasant smell similar to that of anise seed. It is one of three isomers of bromoanisole, the others being 3-bromoanisole and 2-bromoanisole. It is the precursor to many 4-anisyl derivatives.
2-Bromo-4,5-methylenedioxyamphetamine (6-Bromo-MDA) is a lesser-known psychedelic drug and a substituted amphetamine. It was first synthesized by Alexander Shulgin. In his book PiHKAL, the dose is listed as 350 mg and the duration unknown. [1] It produces stimulant effects but with no psychedelic or empathogenic action. [1]
Bromoform was discovered in 1832 by Löwig who distilled a mixture of bromal and potassium hydroxide, as analogous to preparation of chloroform from chloral. [5]Bromoform can be prepared by the haloform reaction using acetone and sodium hypobromite, by the electrolysis of potassium bromide in ethanol, or by treating chloroform with aluminium bromide.
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Methoxytoluenes (methylanisoles or cresyl methyl ethers) are a group of three isomeric organic compounds with the formula CH 3 OC 6 H 4 CH 3. They consist of a disubstituted benzene ring with methoxy group and one methyl group. All three are colorless flammable liquids which are soluble in organic solvents but poorly soluble in water.
The most commonly employed Sandmeyer reactions are the chlorination, bromination, cyanation, and hydroxylation reactions using CuCl, CuBr, CuCN, and Cu 2 O, respectively. More recently, trifluoromethylation of diazonium salts has been developed and is referred to as a 'Sandmeyer-type' reaction.