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Dry distillation is the heating of solid materials to produce gaseous products (which may condense into liquids or solids). The method may involve pyrolysis or thermolysis, or it may not (for instance, a simple mixture of ice and glass could be separated without breaking any chemical bonds, but organic matter contains a greater diversity of molecules, some of which are likely to break).
A McCabe–Thiele diagram for the distillation of a binary (two-component) feed is constructed using the vapor-liquid equilibrium (VLE) data—which is how vapor is concentrated when in contact with its liquid form—for the component with the lower boiling point. Figure 1: Typical McCabe–Thiele diagram for distillation of a binary feed
A copper retort A glass retort. In a chemistry laboratory, a retort is a device used for distillation or dry distillation of substances. It consists of a spherical vessel with a long downward-pointing neck.
Dry distillation (thermolysis and pyrolysis) is the heating of solid materials to produce gases that condense either into fluid products or into solid products. The term dry distillation includes the separation processes of destructive distillation and of chemical cracking, breaking down large hydrocarbon molecules into smaller hydrocarbon ...
As early as the 1920s, the concept of using hot water and alkali catalysts to produce oil out of biomass was proposed. [6] In 1939, U.S. patent 2,177,557, [7] described a two-stage process in which a mixture of water, wood chips, and calcium hydroxide is heated in the first stage at temperatures in a range of 220 to 360 °C (428 to 680 °F), with the pressure "higher than that of saturated ...
The dry distillation of wood remained the major source of methanol into the early 20th century. [16] Pyrolysis was instrumental in the discovery of many chemical substances, such as phosphorus from ammonium sodium hydrogen phosphate NH 4 NaHPO 4 in concentrated urine , oxygen from mercuric oxide , and various nitrates .
Fractionation is widely employed in many branches of science and technology. Mixtures of liquids and gasses are separated by fractional distillation by difference in boiling point. Fractionation of components also takes place in column chromatography by a difference in affinity between stationary phase and the mobile phase .
Pyrolysis oil, sometimes also known as biocrude or bio-oil, is a synthetic fuel with few industrial application and under investigation as substitute for petroleum.It is obtained by heating dried biomass without oxygen in a reactor at a temperature of about 500 °C (900 °F) with subsequent cooling, separation from the aqueous phase and other processes.