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The diagram shows a typical reflux apparatus. It includes a water bath to indirectly heat the mixture. As many solvents used are flammable, direct heating with a Bunsen burner is not generally suitable, and alternatives such as a water bath, oil bath, sand bath, electric hot plate or heating mantle are employed. [6]
A Soxhlet extractor is a piece of laboratory apparatus [1] invented in 1879 by Franz von Soxhlet. [2] It was originally designed for the extraction of a lipid from a solid material. Typically, Soxhlet extraction is used when the desired compound has a limited solubility in a solvent , and the impurity is insoluble in that solvent.
Liebig condenser. The Liebig condenser (/ ˈ l iː b ɪ ɡ /, LEE-big) [1] or straight condenser is a piece of laboratory equipment, specifically a condenser consisting of a straight glass tube surrounded by a water jacket.
In chemistry, a condenser is laboratory apparatus used to condense vapors – that is, turn them into liquids – by cooling them down. [1] Condensers are routinely used in laboratory operations such as distillation, reflux, and extraction. In distillation, a mixture is heated until the more volatile components boil off, the vapors are ...
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The augers themselves frequently contain passages for the heating medium to increase the heat transfer surface area. Some systems use electric resistance heaters instead of a heat transfer media and may employ a single auger in each housing. The augers can range from 12 to 36 inches in diameter for full-scale systems, with lengths up to 20 feet.
Heating an ideal mixture of two volatile substances, A and B, with A having the higher volatility, or lower boiling point, in a batch distillation setup (such as in an apparatus depicted in the opening figure) until the mixture is boiling results in a vapor above the liquid that contains a mixture of A and B.
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