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Pulse electrolysis is an alternate electrolysis method that utilises a pulsed direct current to initiate non-spontaneous chemical reactions. [1] [2] [3] Also known as pulsed direct current (PDC) electrolysis, the increased number of variables that it introduces to the electrolysis method can change the application of the current to the electrodes and the resulting outcome.
Electrolysis is the passing of a direct electric current through an electrolyte which is producing chemical reactions at the electrodes and decomposition of the materials. The main components required to achieve electrolysis are an electrolyte, electrodes, and an external power source.
where Δi p is the differential current peak value, A is the surface area of the electrode, C 0 * is the concentration of the species, D 0 is the diffusivity of the species, t p is the pulse width, and ΔΨ p is a dimensionless parameter which gauges the peak height in SWV relative to the limiting response in normal pulse voltammetry. [4]
Differential pulse voltammetry: An electrochemical technique similar to normal pulse voltammetry but the applied base potential is increased or decreased steadily, and the pulse height: base height ratio is kept constant. In DPV, measurements of current are taken twice during each drop, first immediately before the pulse and second before the ...
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Cathodic stripping voltammetry is a voltammetric method for quantitative determination of specific ionic species. [6] It is similar to the trace analysis method anodic stripping voltammetry, except that for the plating step, the potential is held at an oxidizing potential, and the oxidized species are stripped from the electrode by sweeping the potential negatively.
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