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This still had a pot still type-kettle, but replaced the traditional lyne arm and cooling worm with a vertical column of perforated plates. [7] Although many of the details of Cellier-Blumenthal's column were improved upon in later years, the general concept was to provide the basis for future column still designs. [ 5 ]
The result was more efficient, producing a lighter spirit at higher alcohol content. Coffey patented his design in 1830, and it became the basis for every column still used ever since. His column still became widely popular in Scotland and the rest of the world outside Ireland, where it is known as the "Coffey still" or "Patent Still".
The modern, triple column still at the Belmopan distillery owned by the Perdomo family, Travellers Liquors, Belize. Photo credit-Dan Carey You cannot overwrite this file.
Image 1: Typical industrial distillation towers Image 2: A crude oil vacuum distillation column as used in oil refineries. Continuous distillation, a form of distillation, is an ongoing separation in which a mixture is continuously (without interruption) fed into the process and separated fractions are removed continuously as output streams.
English: Prohibition-era copper still pot, column, and condenser (c. 1920). From the collection of the McCleary Historical Museum, McCleary, Washington. Photo taken at "Stills in the Hills", a 2012 exhibit about bootlegging during the Prohibition era in the United States, at White River Valley Museum, Auburn, Washington.
The hot crude oil is then passed into a distillation column that allows the separation of the crude oil into different fractions depending on the difference in volatility. The pressure at the top is maintained at 1.2–1.5 atm [ 2 ] so that the distillation can be carried out at close to atmospheric pressure, and therefore it is known as the ...
Still's innovation was to apply pressure to the top of the column to increase the speed of solvent elution. Not only did this drastically reduce the time required to run the column, but it also allowed for the routine separation of compounds having an R f difference of 0.10 or greater. After optimizing this procedure, Still compiled a table ...
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