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The diagram shows a typical reflux apparatus. It includes a water bath to indirectly heat the mixture. As many solvents used are flammable, direct heating with a Bunsen burner is not generally suitable, and alternatives such as a water bath, oil bath, sand bath, electric hot plate or heating mantle are employed. [6]
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Date/Time Thumbnail Dimensions User Comment; current: 01:02, 12 November 2009: 350 × 575 (13 KB): Andrew c (This is a diagram of a en:reflux apparatus with English labels.
A Soxhlet extractor is a piece of laboratory apparatus [1] invented in 1879 by Franz von Soxhlet. [2] It was originally designed for the extraction of a lipid from a solid material. Typically, Soxhlet extraction is used when the desired compound has a limited solubility in a solvent , and the impurity is insoluble in that solvent.
A Perkin triangle is a specialized apparatus for the distillation of air-sensitive materials. Some compounds have high boiling points and are sensitive to air. A simple vacuum distillation system can be used, whereby the vacuum is replaced with an inert gas after the distillation is complete. However, this is a less satisfactory system if one ...
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Cutaway sections show heating elements around the bowl containing sand. A sand bath is a common piece of laboratory equipment made from a container filled with heated sand. It is used to evenly heat another container, most often during a chemical reaction. A sand bath is most commonly used in conjunction with a hot plate or heating mantle.