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The Trapp mixture is a specific mixture of organic solvents that allows chemical reactions to take place at very low temperatures. [1] It is made up of THF:diethyl ether:pentane in a 4:4:1 ratio which remains liquid down to −110 °C and the same solvents in a 4:1:1 ratio remain a liquid down to −120 °C.
A flame arrester during testing A flame arrester made for a 91 cm (36 inch) pipe weighing 10 tons. A flame arrester (also spelled arrestor), deflagration arrester, [1] or flame trap [2] is a device or form of construction that will allow free passage of a gas or gaseous mixture but will interrupt or prevent the passage of flame.
The inert-gas line is vented through an oil bubbler, while solvent vapors and gaseous reaction products are prevented from contaminating the vacuum pump by a liquid-nitrogen or dry-ice/acetone cold trap. Special stopcocks or Teflon taps allow vacuum or inert gas to be selected without the need for placing the sample on a separate line. [3]
Liquid oxygen is potentially explosive, and this is especially true if the trap has been used to trap solvent. Oxygen can be condensed into a cold trap if a pump has sucked air through the trap when the trap is very cold, e.g. when cooled with liquid nitrogen .
In chemistry, a chemical trap is a chemical compound that is used to detect unstable compounds. [1] The method relies on efficiency of bimolecular reactions with reagents to produce a more easily characterize trapped product. In some cases, the trapping agent is used in large excess.
A rotary evaporator [1] (rotovap) is a device used in chemical laboratories for the efficient and gentle removal of solvents from samples by evaporation.When referenced in the chemistry research literature, description of the use of this technique and equipment may include the phrase "rotary evaporator", though use is often rather signaled by other language (e.g., "the sample was evaporated ...
SilencerCo Osprey .45 suppressor on a Springfield pistol. SilencerCo was founded in 2008 by former President Jonathon Shults and Joshua Waldron. [3] Soon after, SilencerCo launched its first product, a .22 caliber silencer called the Sparrow. [4]
The signal from the solvent can overwhelm that of the solute, and the NMR instrument may not collect any meaningful data. Solvent suppression techniques are particularly important in protein NMR where the solvent often includes H 2 O as well as D 2 O. [2]