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Schematic diagram of a Michelson interferometer, configured for FTIR. In a Michelson interferometer adapted for FTIR, light from the polychromatic infrared source, approximately a black-body radiator, is collimated and directed to a beam splitter. Ideally 50% of the light is refracted towards the fixed mirror and 50% is transmitted towards the ...
FTIR mode Sample preparation Schematic diagram Transmission FTIR: Transmission mode is the most widely used FTIR technique in geoscience due to its high analysis speed and cost-efficient characteristics. [4] The sample, either a rock or a mineral, is cut into a block and polished on both sides until a thin (typically 300 to 15 μm) wafer is ...
Schematic of a 2D IR spectrum. The red circles correspond to bleaching of the ground state. The blue circles correspond to absorption of the excited state. The smaller off-diagonal circles to coupling between the two states. The linear absorption (FTIR) spectrum is indicated above the 2D IR spectrum.
The schematic representation of a nano-FTIR system with a broadband infrared source. Nano-FTIR (nanoscale Fourier transform infrared spectroscopy) is a scanning probe technique that utilizes as a combination of two techniques: Fourier transform infrared spectroscopy (FTIR) and scattering-type scanning near-field optical microscopy (s-SNOM).
A common laboratory instrument that uses this technique is a Fourier transform infrared (FTIR) spectrometer. Two-dimensional IR is also possible as discussed below. The infrared portion of the electromagnetic spectrum is usually divided into three regions; the near-, mid- and far-infrared, named for their relation to the visible spectrum.
Particularly in nano-FTIR, where the scattering from a sharp probe-tip is used to perform spectroscopy of samples with nanoscale spatial resolution, a high-power illumination from pulsed infrared lasers makes up for a relatively small scattering efficiency (often < 1%) of the probe. [4]
ATR-FTIR is also used as a tool in pharmacological research to investigate protein/pharmaceutical interactions in detail. Water-soluble proteins to be investigated require Polyhistidine-tags , allowing the macromolecule to be anchored to a lipid bilayer, which is attached to a Germanium crystal or other suitable optical media.
Schematic diagram of (1) collection mode and (2) illumination mode The high-quality infrared fiber tip is very important in realizing NSOM/FTIR technique. There are several types of fibers, such as sapphire , chalcogenide glass , fluoride glass and hollow silica guides. [ 53 ]