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The vacuuming is continued for another 2 to 3 minutes to make certain all of the air has been removed from the material. Once this interval is reached, the vacuum pump is shut off and the vacuum chamber release valve is opened to equalize air pressure. The vacuum chamber is opened, the material is removed and is ready to pour into the mold.
1 Cooling water in 2 Cooling water out 3 Vacuum/gas line 4 Sublimation chamber 5 Sublimed compound 6 Crude material 7 External heating A sublimatory [ 1 ] [ 2 ] or sublimation apparatus is equipment, commonly laboratory glassware , for purification of compounds by selective sublimation .
The 1698 van Musschenbroek vacuum pump at Museum Boerhaave, before it was moved to the University Museum of Groningen. The pump contains a chamber, a diagonal barrel and a main house with four spanners. All are connected to a wooden base. Turning the spanners counter-clockwise will pull up the piston and create vacuum in the barrel.
Vacuum systems usually consist of gauges, vapor jet and pumps, vapor traps and valves along with other extensional piping. A vessel that is operating under vacuum system may be any of these types such as processing tank, steam simulator, particle accelerator, or any other type of space that has an enclosed chamber to maintain the system in less than atmospheric gas pressure.
The device consists of a perforated table top containing a vacuum chamber, and a vacuum pump to keep the vacuum chamber below ambient enough pressure. The workpiece is placed on the top of the vacuum chamber and thus held down by the pressure differential between the vacuum chamber and the outside air.
A better choice for vacuum systems is the tin-silver eutectic, Sn95Ag5 (Sn-Ag eutectic is actually 96.5-3.5); its melting point of 230 °C (446 °F) allows bakeout up to 200 °C (392 °F). A similar 95-5 alloy, Sn95Sb5, is unsuitable as antimony has similar vapor pressure as lead. Take care to remove flux residues.