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Pulse electrolysis is an alternate electrolysis method that utilises a pulsed direct current to initiate non-spontaneous chemical reactions. [1] [2] [3] Also known as pulsed direct current (PDC) electrolysis, the increased number of variables that it introduces to the electrolysis method can change the application of the current to the electrodes and the resulting outcome.
Electrolysis is the passing of a direct electric current through an electrolyte which is producing chemical reactions at the electrodes and decomposition of the materials. The main components required to achieve electrolysis are an electrolyte, electrodes, and an external power source.
Differential pulse voltammetry: An electrochemical technique similar to normal pulse voltammetry but the applied base potential is increased or decreased steadily, and the pulse height: base height ratio is kept constant. In DPV, measurements of current are taken twice during each drop, first immediately before the pulse and second before the ...
where Δi p is the differential current peak value, A is the surface area of the electrode, C 0 * is the concentration of the species, D 0 is the diffusivity of the species, t p is the pulse width, and ΔΨ p is a dimensionless parameter which gauges the peak height in SWV relative to the limiting response in normal pulse voltammetry. [4]
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This is typically electrolysis of water, which generates hydrogen peroxide, hydrogen ions (acid) and hydroxide (base) as well as oxygen and hydrogen gas bubbles. The hydrogen peroxide and/or pH changes generated can adversely affect biological cells and biomolecules such as proteins, while gas bubbles tend to "clog" microfluidic systems.
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