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The Cleveland open-cup method is one of three main methods in chemistry for determining the flash point of a petroleum product using a Cleveland open-cup apparatus, also known as a Cleveland open-cup tester. [1] First, the test cup of the apparatus (usually brass) is filled to a certain level with a portion of the product.
The measured flash point will actually vary with the height of the flame above the liquid surface and, at sufficient height, the measured flash point temperature will coincide with the fire point. The best-known example is the Cleveland open cup (COC). [5]
This allows the development of an equilibrium between the liquid and the air volume. The ignition source is directed into the cup at regular intervals with simultaneous interruption of stirring. The test concludes upon observation of a flash that spreads throughout the inside of the cup. The corresponding temperature is the liquid's flash point.
Most tables of material properties will only list material flash points. In general, the fire point can be assumed to be about 10 °C higher than the flash point, [2] although this is no substitute for testing if the fire point is safety critical. [2] Testing of the fire point is done by open cup apparatus. [2] [3]
Smoke point decreases at a different pace in different oils. [10] Considerably above the temperature of the smoke point is the flash point, the point at which the vapours from the oil can ignite in air, given an ignition source. The following table presents smoke points of various fats and oils.
The laser flash method was developed by Parker et al. in 1961. [1] In a vertical setup, a light source (e.g. laser, flashlamp) heats the sample from the bottom side and a detector on top detects the time-dependent temperature rise. For measuring the thermal diffusivity, which is strongly temperature-dependent, at different temperatures the ...
An Orsat gas analyser or Orsat apparatus is a piece of laboratory equipment used to analyse a gas sample (typically fossil fuel flue gas) for its oxygen, carbon monoxide and carbon dioxide content. Although largely replaced by instrumental techniques, the Orsat remains a reliable method of measurement and is relatively simple to use.
A sealed capillary, open end pointing down, is placed in the fusion tube. The Thiele tube is heated; dissolved gases evolve from the sample first. Once the sample starts to boil, heating is stopped, and the temperature starts to fall. The temperature at which the liquid sample is sucked into the sealed capillary is the boiling point of the sample.